USGS-NWQL: I-5399: Lead, recoverable-from-bottom-material, FLAA
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Official Method Name
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Lead, atomic absorption spectrometric, direct |
|---|---|
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Current Revision
| 1985 |
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Media
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SOILS/SEDIMENT |
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Instrumentation
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Flame Atomic Absorption |
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Method Subcategory
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Inorganic |
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Method Source
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|
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Citation
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Methods for the Determination of Inorganic Substances in Water and Fluvial Sediments, Techniques of Water-Resources Investigations of the United States Geological Survey, Book 5, Chapter A1 Edited by Marvin J. Fishman and Linda C. Friedman |
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Brief Method Summary
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Lead is determined by flame atomic absorption spectrometry by direct aspiration of the sample solution into an air-acetylene flame. |
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Scope and Application
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This method may be used to analyze bottom material containing at least 10 ug/g of lead. Prepared sample solutions containing more than 4,000ug/L need either to be diluted or to be read on a less expanded scale. Recoverable lead in bottom material needs to undergo preliminary digestion-solubilization by method I-5485 before being determined. |
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Applicable Concentration Range
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at least 10 ug/g of lead |
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Interferences
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Individual concentrations of sodium (9,000 mg/L), potassium (9,000 mg/L), calcium (4,000 mg/L), magnesium (4,000 mg/L), nitrate (900 mg/L), iron (4 X 106 ug/L), and cadmium, nickel, copper, zinc, cobalt, and chromium (10,000 ug/L) do not interfere. Higher concentrations of each constituent were not investigated. |
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Quality Control Requirements
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Calibrate instrument using calibration standards (CAL). Quality control samples (QCS) and laboratory blanks (LB) analyzed at a minimum of I each after every 10 samples |
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Sample Handling
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Container Description: 500 mL Polypropylene bottle, wide-mouth. Treatment and Preservation: No treatment, preservation or special shipping requirements |
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Maximum Holding Time
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180 days |
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Relative Cost
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Less than $50 |
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Sample Preparation Methods
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I-5485 |
