DOE EML: Se-03:  Americium, Plutonium and Uranium in Water

  • Summary
  • Analytes
  • Revision
  • Data and Sites
Official Method Name
Sequential Analysis - AMERICIUM, PLUTONIUM AND URANIUM IN WATER
Current Revision
EML Procedures Manual HASL-300, Volume 1, 28th Ed.(1997)
Media
WATER
Instrumentation
Alpha Spectrometer/Counter
Method Subcategory
Radiochemical
Method Source
  DOE EML
Citation
  DOE EML Procedures Manual HASL-300, Volume 1, 28th Ed.(1997)
Brief Method Summary
Americium, plutonium and uranium are separated by Eichrom resins prior to measurements by alpha spectrometry. Tracers are used to monitor chemical recoveries and to correct the results to improve precision and accuracy. This is a rapid, reliable method for the measurement of actinides in water samples that is more cost-effective and efficient than traditional ion exchange, solvent extraction and precipitation techniques.
The method is adapted from Eichrom Industries, Inc., Procedure ACW03, Rev. 1.5.
Scope and Application
This procedure describes a method for the separation and measurement of americium, plutonium and uranium in water.
Applicable Concentration Range
None given.
Interferences
(A) Unresolvable alpha energies - Actinides with unresolvable alpha energies such as Am-241 and Pu-238 or Np-237 and U-234 must be chemically separated to enable measurement. This method effectively separates these isotopes.
Quality Control Requirements
Sample Handling
None given.
Maximum Holding Time
None given.
Relative Cost
$51 to $200
Sample Preparation Methods
G-03