EPA-RCA: 8270D: Semivolatile Organic Compounds by GC/MS
- Summary
- Analytes
- Revision
- Data and Sites
Official Method Name
|
Semivolatile Organic Compounds by GC/MS | ||||
---|---|---|---|---|---|
Current Revision
| Revision 4.0, January 1998 | ||||
Media
|
VARIOUS | ||||
Instrumentation
|
Gas Chromatography with Mass Spectrometry Detection | ||||
Method Subcategory
|
Organic | ||||
Method Source
|
EPA-RCA
|
||||
Citation
|
SW-846 Update IVA
|
||||
Brief Method Summary
|
The samples are prepared for analysis by gas chromatography/mass spectrometry (GC/MS) using the appropriate sample preparation (refer to Method 3500) and, if necessary, sample cleanup procedures (refer to Method 3600). The semivolatile compounds are introduced into the GC/MS by injecting the sample extract into a gas chromatograph (GC) with a narrow-bore fused-silica capillary column. The GC column is temperature-programmed to separate the analytes, which are then detected with a mass spectrometer (MS) connected to the gas chromatograph. Analytes eluted from the capillary column are introduced into the mass spectrometer via a jet separator or a direct connection. Identification of target analytes is accomplished by comparing their mass spectra with the electron impact (or electron impact-like) spectra of authentic standards. Quantitation is accomplished by comparing the response of a major (quantitation) ion relative to an internal standard using a five-point calibration curve. NOTE: This method can be used in conjunction with the following sample preparation procedures: Air (particulates and sorbent resin)- Method 3542 Water (including TCLP leachates) - Methods 3510, 3520, 3535 Soil/sediment - Methods 3540, 3541, 3545, 3546 3550, 3560, 3561 Waste - Methods 3540, 3541, 3545, 3546, 3550, 3560, 3561, 3580 |
||||
Scope and Application
|
Method 8270 is used to determine the concentration of semivolatile organic compounds in extracts prepared from many types of solid waste matrices, soils, air sampling media and water samples. Direct injection of a sample may be used in limited applications. | ||||
Applicable Concentration Range
|
None given. | ||||
Interferences
|
(1) Contaminants from glassware. (2) Matrix interferences that are co-extracted with sample. (3) Contamination by carryover can occur whenever high-concentration and low-concentration samples are sequentially analyzed. To reduce carryover, the sample syringe must be rinsed with solvent between sample injections. Whenever an unusually concentrated sample is encountered, it should be followed by the analysis of solvent to check for cross-contamination. |
||||
Quality Control Requirements
|
See SW-846 Method 8000 and 3500. Procedures include: validation of sample preparation, introduction, and analysis, initial demonstration of proficiency, calibration verification, evaluation of retention times, analysis of method blanks, matrix spikes, duplicates, surrogates, and laboratory control samples. | ||||
Sample Handling
|
Store the extract at 4 degrees C, protected from light in screw-cap vials equipped with unpierced Teflon lined septa. See SW-846, Chapter 4, Organic Analytes, Section 4.1. See SW-846 Chapter Four for information. | ||||
Maximum Holding Time
|
Aqueous samples - 7 days (sample), 40 days (extract). Solid samples - 14 days (sample), 40 (extract). Also, see SW-846 Chapter Four for information. | ||||
Relative Cost
|
$201 to $400 | ||||
Sample Preparation Methods
|
See Method Summary |
This method has 248 analytes associated with it.
Analyte | Detection Level |
Bias | Precision | Pct False Positive |
Pct False Negative |
Spiking Level |
---|---|---|---|---|---|---|
1,2,4,5-Tetrachlorobenzene(95-94-3)
|
10.000 ug/L | N/A | N/A | |||
1,2,4-Trichlorobenzene(120-82-1)
|
10.000 ug/L | 92% Rec (ML) | 21.78 % RSD (ML) | 50.00 ug/L | ||
1,2-Dichlorobenzene(95-50-1)
|
10.000 ug/L | 81% Rec (ML) | 24.78 % RSD (ML) | 50.00 ug/L | ||
1,2-Dinitrobenzene(528-29-0)
|
40.000 ug/L | N/A | N/A | |||
1,2-Diphenylhydrazine(122-66-7)
|
N/A | N/A | N/A | |||
1,3-Dichlorobenzene(541-73-1)
|
10.000 ug/L | 85% Rec (ML) | 41.22 % RSD (ML) | 50.00 ug/L | ||
1,3-Dinitrobenzene(99-65-0)
|
20.000 ug/L | N/A | N/A | |||
1,4-Dichlorobenzene(106-46-7)
|
10.000 ug/L | 70% Rec (ML) | 29.72 % RSD (ML) | 50.00 ug/L | ||
1,4-Dinitrobenzene(100-25-4)
|
40.000 ug/L | N/A | N/A | |||
1,4-Naphthoquinone(130-15-4)
|
10.000 ug/L | N/A | N/A | |||
1-Acetyl-2-thiourea(591-08-2)
|
1000.000 ug/L | N/A | N/A | |||
1-Chloronaphthalene(90-13-1)
|
N/A | N/A | N/A | |||
2,3,4,6-Tetrachlorophenol(58-90-2)
|
10.000 ug/L | N/A | N/A | |||
2,4,5-Trichlorophenol(95-95-4)
|
20.000 ug/L | N/A | N/A | |||
2,4,5-Trimethylaniline(137-17-7)
|
10.000 ug/L | N/A | N/A | |||
2,4,6-Trichlorophenol(88-06-2)
|
10.000 ug/L | 91% Rec (ML) | 25.62 % RSD (ML) | 50.00 ug/L | ||
2,4-Diaminotoluene(95-80-7)
|
10.000 ug/L | N/A | N/A | |||
2,4-Dichlorophenol(120-83-2)
|
10.000 ug/L | 87% Rec (ML) | 23.56 % RSD (ML) | 50.00 ug/L | ||
2,4-Dimethylphenol(105-67-9)
|
10.000 ug/L | 80% Rec (ML) | 24.62 % RSD (ML) | 50.00 ug/L | ||
2,4-Dinitrophenol(51-28-5)
|
50.000 ug/L | 45% Rec (ML) | 94.58 % RSD (ML) | 50.00 ug/L | ||
2,4-Dinitrotoluene(121-14-2)
|
10.000 ug/L | 82% Rec (ML) | 24.00 % RSD (ML) | 50.00 ug/L | ||
2,6-Dichlorophenol(87-65-0)
|
10.000 ug/L | N/A | N/A | |||
2,6-Dinitrotoluene(606-20-2)
|
10.000 ug/L | 99% Rec (ML) | 19.70 % RSD (ML) | 50.00 ug/L | ||
2-Aminoanthraquinone(117-79-3)
|
20.000 ug/L | N/A | N/A | |||
2-Chloronaphthalene(91-58-7)
|
10.000 ug/L | 89% Rec (ML) | 13.68 % RSD (ML) | 50.00 ug/L | ||
2-Chlorophenol(95-57-8)
|
10.000 ug/L | 79% Rec (ML) | 29.94 % RSD (ML) | 50.00 ug/L | ||
2-Methyl-4,6-dinitrophenol(534-52-1)
|
N/A | N/A | N/A | |||
2-Methylnaphthalene(91-57-6)
|
10.000 ug/L | N/A | N/A | |||
2-Nitroaniline(88-74-4)
|
50.000 ug/L | N/A | N/A | |||
2-Nitrophenol(88-75-5)
|
10.000 ug/L | 105% Rec (ML) | 32.20 % RSD (ML) | 50.00 ug/L | ||
3,3'-Dichlorobenzidine(91-94-1)
|
20.000 ug/L | 98% Rec (ML) | 53.90 % RSD (ML) | 50.00 ug/L | ||
3,3'-Dimethoxybenzidine(119-90-4)
|
100.000 ug/L | N/A | N/A | |||
3-Amino-9-ethyl carbazole(132-32-1)
|
N/A | N/A | N/A | |||
3-Methylcholanthrene(56-49-5)
|
10.000 ug/L | N/A | N/A | |||
3-Nitroaniline(99-09-2)
|
50.000 ug/L | N/A | N/A | |||
4,4'-DDD(72-54-8)
|
N/A | 55% Rec (ML) | 64.08 % RSD (ML) | 50.00 ug/L | ||
4,4'-DDE(72-55-9)
|
N/A | 69% Rec (ML) | 36.92 % RSD (ML) | 50.00 ug/L | ||
4,4'-Methylenebis(2-chloroaniline)(101-14-4)
|
N/A | N/A | N/A | |||
4,4'-Methylenebis(N,N-dimethyl) benzenamine(101-61-1)
|
N/A | N/A | N/A | |||
4,4'-Oxydianiline(101-80-4)
|
20.000 ug/L | N/A | N/A | |||
4-Aminobiphenyl(92-67-1)
|
20.000 ug/L | N/A | N/A | |||
4-Bromophenyl phenyl ether(101-55-3)
|
10.000 ug/L | 88% Rec (ML) | 17.32 % RSD (ML) | 50.00 ug/L | ||
4-Chloro-3-methylphenol(59-50-7)
|
N/A | N/A | N/A | |||
4-Chloro-m-phenylenediamine(5131-60-2)
|
N/A | N/A | N/A | |||
4-Chloro-o-phenylenediamine(95-83-0)
|
N/A | N/A | N/A | |||
4-Chlorophenylphenyl ether(7005-72-3)
|
10.000 ug/L | 92% Rec (ML) | 29.08 % RSD (ML) | 50.00 ug/L | ||
4-Nitrobiphenyl(92-93-3)
|
10.000 ug/L | N/A | N/A | |||
4-Nitrophenol(100-02-7)
|
10.000 ug/L | 59% Rec (ML) | 50.48 % RSD (ML) | 50.00 ug/L | ||
4-Nitroquinoline-1-oxide(56-57-5)
|
40.000 ug/L | N/A | N/A | |||
5-Chloro-o-toluidine(95-79-4)
|
N/A | N/A | N/A | |||
5-Nitro-o-anisidine(99-59-2)
|
10.000 ug/L | N/A | N/A | |||
5-Nitro-o-toluidine(99-55-8)
|
N/A | N/A | N/A | |||
5-Nitroacenaphthene(602-87-9)
|
10.000 ug/L | N/A | N/A | |||
7,12-Dimethylbenz(a)anthracene(57-97-6)
|
10.000 ug/L | N/A | N/A | |||
Acenaphthene(83-32-9)
|
10.000 ug/L | 96% Rec (ML) | 19.66 % RSD (ML) | 50.00 ug/L | ||
Acenaphthylene(208-96-8)
|
10.000 ug/L | 90% Rec (ML) | 24.92 % RSD (ML) | 50.00 ug/L | ||
Acetamidofluorene(53-96-3)
|
20.000 ug/L | N/A | N/A | |||
Acetophenone(98-86-2)
|
10.000 ug/L | N/A | N/A | |||
Aldrin(309-00-2)
|
N/A | 81% Rec (ML) | 45.26 % RSD (ML) | 50.00 ug/L | ||
Aminoazobenzene(60-09-3)
|
10.000 ug/L | N/A | N/A | |||
Anilazine(101-05-3)
|
100.000 ug/L | N/A | N/A | |||
Aniline(62-53-3)
|
N/A | N/A | N/A | |||
Anthracene(120-12-7)
|
N/A | 81% Rec (ML) | 25.72 % RSD (ML) | 50.00 ug/L | ||
Aramite(140-57-8)
|
20.000 ug/L | N/A | N/A | |||
Azinphos-methyl(86-50-0)
|
100.000 ug/L | N/A | N/A | |||
Barban(101-27-9)
|
200.000 ug/L | N/A | N/A | |||
Benz[a]anthracene(56-55-3)
|
10.000 ug/L | 87% Rec (ML) | 25.44 % RSD (ML) | 50.00 ug/L | ||
Benzenethiol(108-98-5)
|
N/A | N/A | N/A | |||
Benzidine(92-87-5)
|
N/A | N/A | N/A | |||
Benzo(a)pyrene(50-32-8)
|
N/A | 90% Rec (ML) | 34.70 % RSD (ML) | 50.00 ug/L | ||
Benzo(b)fluoranthene(205-99-2)
|
10.000 ug/L | 89% Rec (ML) | 30.92 % RSD (ML) | 50.00 ug/L | ||
Benzo(g,h,i)perylene(191-24-2)
|
10.000 ug/L | 96% Rec (ML) | 50.12 % RSD (ML) | 50.00 ug/L | ||
Benzo(k)fluoranthene(207-08-9)
|
10.000 ug/L | 84% Rec (ML) | 35.80 % RSD (ML) | 50.00 ug/L | ||
Benzoic acid(65-85-0)
|
50.000 ug/L | N/A | N/A | |||
Benzyl alcohol(100-51-6)
|
20.000 ug/L | N/A | N/A | |||
Bromoxynil(1689-84-5)
|
10.000 ug/L | N/A | N/A | |||
Butyl benzyl phthalate(85-68-7)
|
10.000 ug/L | 63% Rec (ML) | 54.84 % RSD (ML) | 50.00 ug/L | ||
Captan(133-06-2)
|
50.000 ug/L | N/A | N/A | |||
Carbamate pesticides(E-12895)
|
N/A | N/A | N/A | |||
Carbaryl(63-25-2)
|
N/A | N/A | N/A | |||
Carbofuran(1563-66-2)
|
10.000 ug/L | N/A | N/A | |||
Carbophenothion(786-19-6)
|
10.000 ug/L | N/A | N/A | |||
Chlordane(57-74-9)
|
N/A | N/A | N/A | |||
Chlorfenvinphos(470-90-6)
|
20.000 ug/L | N/A | N/A | |||
Chlorobenzilate(510-15-6)
|
10.000 ug/L | N/A | N/A | |||
Chrysene(218-01-9)
|
10.000 ug/L | 91% Rec (ML) | 32.82 % RSD (ML) | 50.00 ug/L | ||
Coumaphos(56-72-4)
|
40.000 ug/L | N/A | N/A | |||
Crotoxyphos(7700-17-6)
|
20.000 ug/L | N/A | N/A | |||
DBCP(96-12-8)
|
N/A | N/A | N/A | |||
Demeton-O(298-03-3)
|
10.000 ug/L | N/A | N/A | |||
Demeton-S(126-75-0)
|
10.000 ug/L | N/A | N/A | |||
Di-n-butyl phthalate(84-74-2)
|
10.000 ug/L | 60% Rec (ML) | 40.20 % RSD (ML) | 50.00 ug/L | ||
Di-n-octyl phthalate(117-84-0)
|
10.000 ug/L | 74% Rec (ML) | 39.38 % RSD (ML) | 50.00 ug/L | ||
Diallate(2303-16-4)
|
10.000 ug/L | N/A | N/A | |||
Dibenz(a,j)acridine(224-42-0)
|
10.000 ug/L | N/A | N/A | |||
Dibenzo(a,e)pyrene(192-65-4)
|
10.000 ug/L | N/A | N/A | |||
Dibenzo(a,h)anthracene(53-70-3)
|
N/A | 97% Rec (ML) | 59.50 % RSD (ML) | 50.00 ug/L | ||
Dibenzofuran(132-64-9)
|
10.000 ug/L | N/A | N/A | |||
Dichlone(117-80-6)
|
N/A | N/A | N/A | |||
Dichlorvos(62-73-7)
|
10.000 ug/L | N/A | N/A | |||
Dicrotophos(141-66-2)
|
10.000 ug/L | N/A | N/A | |||
Dieldrin(60-57-1)
|
N/A | 82% Rec (ML) | 25.86 % RSD (ML) | 50.00 ug/L | ||
Diethyl phthalate(84-66-2)
|
10.000 ug/L | 45% Rec (ML) | 52.44 % RSD (ML) | 50.00 ug/L | ||
Diethylstilbestrol(56-53-1)
|
20.000 ug/L | N/A | N/A | |||
Diethylsulfate(64-67-5)
|
100.000 ug/L | N/A | N/A | |||
Dihydrosafrole(94-58-6)
|
N/A | N/A | N/A | |||
Dilantin(57-41-0)
|
N/A | N/A | N/A | |||
Dimethoate(60-51-5)
|
20.000 ug/L | N/A | N/A | |||
Dimethyl phthalate(131-11-3)
|
10.000 ug/L | 30% Rec (ML) | 95.80 % RSD (ML) | 10.00 ug/L | ||
Dinex(131-89-5)
|
N/A | N/A | N/A | |||
Dinocap(39300-45-3)
|
100.000 ug/L | N/A | N/A | |||
Dinoseb(88-85-7)
|
20.000 ug/L | N/A | N/A | |||
Dioxathion(78-34-2)
|
N/A | N/A | N/A | |||
Diphenylamine(122-39-4)
|
N/A | N/A | N/A | |||
Disulfoton(298-04-4)
|
10.000 ug/L | N/A | N/A | |||
EPN(2104-64-5)
|
10.000 ug/L | N/A | N/A | |||
Endosulfan sulfate(1031-07-8)
|
N/A | 41% Rec (ML) | 57.85 % RSD (ML) | 20.00 ug/L | ||
Endosulfan-I(959-98-8)
|
N/A | N/A | N/A | |||
Endosulfan-II(33213-65-9)
|
N/A | N/A | N/A | |||
Endrin(72-20-8)
|
N/A | N/A | N/A | |||
Endrin aldehyde(7421-93-4)
|
N/A | 68% Rec (ML) | 71.76 % RSD (ML) | 50.00 ug/L | ||
Endrin ketone(53494-70-5)
|
N/A | N/A | N/A | |||
Ethion(563-12-2)
|
10.000 ug/L | N/A | N/A | |||
Ethyl methanesulfonate(62-50-0)
|
20.000 ug/L | N/A | N/A | |||
Ethyl parathion(56-38-2)
|
10.000 ug/L | N/A | N/A | |||
Famphur(52-85-7)
|
20.000 ug/L | N/A | N/A | |||
Fensulfothion(115-90-2)
|
40.000 ug/L | N/A | N/A | |||
Fenthion(55-38-9)
|
10.000 ug/L | N/A | N/A | |||
Fluchloralin(33245-39-5)
|
20.000 ug/L | N/A | N/A | |||
Fluoranthene(206-44-0)
|
10.000 ug/L | 83% Rec (ML) | 26.80 % RSD (ML) | 50.00 ug/L | ||
Fluorene(86-73-7)
|
10.000 ug/L | 90% Rec (ML) | 14.22 % RSD (ML) | 50.00 ug/L | ||
HN-1(538-07-8)
|
N/A | N/A | N/A | |||
HN-3(555-77-1)
|
N/A | N/A | N/A | |||
Heptachlor(76-44-8)
|
N/A | 81% Rec (ML) | 49.54 % RSD (ML) | 50.00 ug/L | ||
Heptachlor epoxide(1024-57-3)
|
N/A | 88% Rec (ML) | 29.28 % RSD (ML) | 50.00 ug/L | ||
Herbicides(E-12839)
|
N/A | N/A | N/A | |||
Hexachlorobenzene(118-74-1)
|
10.000 ug/L | 75% Rec (ML) | 41.96 % RSD (ML) | 50.00 ug/L | ||
Hexachlorobutadiene(87-68-3)
|
10.000 ug/L | 69% Rec (ML) | 26.98 % RSD (ML) | 50.00 ug/L | ||
Hexachlorocyclopentadiene(77-47-4)
|
10.000 ug/L | N/A | N/A | |||
Hexachloroethane(67-72-1)
|
10.000 ug/L | 71% Rec (ML) | 18.60 % RSD (ML) | 50.00 ug/L | ||
Hexachlorophene(70-30-4)
|
50.000 ug/L | N/A | N/A | |||
Hexachloropropene(1888-71-7)
|
10.000 ug/L | N/A | N/A | |||
Hexamethylphosphoramide(680-31-9)
|
20.000 ug/L | N/A | N/A | |||
Hydroquinone(123-31-9)
|
N/A | N/A | N/A | |||
Indeno(1,2,3-cd)pyrene(193-39-5)
|
10.000 ug/L | 72% Rec (ML) | 50.88 % RSD (ML) | 50.00 ug/L | ||
Isodrin(465-73-6)
|
20.000 ug/L | N/A | N/A | |||
Isophorone(78-59-1)
|
10.000 ug/L | 115% Rec (ML) | 33.52 % RSD (ML) | 50.00 ug/L | ||
Isosafrole(120-58-1)
|
10.000 ug/L | N/A | N/A | |||
Kepone(143-50-0)
|
20.000 ug/L | N/A | N/A | |||
Leptophos(21609-90-5)
|
10.000 ug/L | N/A | N/A | |||
Lindane(58-89-9)
|
N/A | N/A | N/A | |||
Malathion(121-75-5)
|
50.000 ug/L | N/A | N/A | |||
Maleic anhydride(108-31-6)
|
N/A | N/A | N/A | |||
Mestranol(72-33-3)
|
20.000 ug/L | N/A | N/A | |||
Methapyrilene(91-80-5)
|
100.000 ug/L | N/A | N/A | |||
Methoxychlor(72-43-5)
|
N/A | N/A | N/A | |||
Methyl methanesulfonate(66-27-3)
|
10.000 ug/L | N/A | N/A | |||
Methyl parathion(298-00-0)
|
10.000 ug/L | N/A | N/A | |||
Mevinphos(7786-34-7)
|
10.000 ug/L | N/A | N/A | |||
Mexacarbate(315-18-4)
|
20.000 ug/L | N/A | N/A | |||
Mirex(2385-85-5)
|
10.000 ug/L | N/A | N/A | |||
Monocrotophos(6923-22-4)
|
40.000 ug/L | N/A | N/A | |||
N-Nitrosodiphenylamine(86-30-6)
|
10.000 ug/L | N/A | N/A | |||
N-Nitrosomorpholine(59-89-2)
|
N/A | N/A | N/A | |||
NDBA(924-16-3)
|
10.000 ug/L | N/A | N/A | |||
NDEA(55-18-5)
|
20.000 ug/L | N/A | N/A | |||
NDMA(62-75-9)
|
N/A | N/A | N/A | |||
NDPA(621-64-7)
|
N/A | 100% Rec (ML) | 44.94 % RSD (ML) | 50.00 ug/L | ||
NMEA(10595-95-6)
|
N/A | N/A | N/A | |||
NPIP(100-75-4)
|
20.000 ug/L | N/A | N/A | |||
NPYR(930-55-2)
|
40.000 ug/L | N/A | N/A | |||
Naled(300-76-5)
|
20.000 ug/L | N/A | N/A | |||
Naphthalene(91-20-3)
|
10.000 ug/L | 79% Rec (ML) | 28.64 % RSD (ML) | 50.00 ug/L | ||
Nicotine(54-11-5)
|
20.000 ug/L | N/A | N/A | |||
Nitrobenzene(98-95-3)
|
10.000 ug/L | 103% Rec (ML) | 27.42 % RSD (ML) | 50.00 ug/L | ||
Nitrofen(1836-75-5)
|
20.000 ug/L | N/A | N/A | |||
O,O,O-Triethylphosphorothioate(126-68-1)
|
N/A | N/A | N/A | |||
Octamethylpyrophosphoramide(152-16-9)
|
200.000 ug/L | N/A | N/A | |||
Organics, semivolatile(E-12884)
|
N/A | N/A | N/A | |||
Organochlorine pesticides(E-12851)
|
N/A | N/A | N/A | |||
Organophosphate pesticides(E-12873)
|
N/A | N/A | N/A | |||
PCB-1016(12674-11-2)
|
N/A | N/A | N/A | |||
PCB-1221(11104-28-2)
|
N/A | N/A | N/A | |||
PCB-1232(11141-16-5)
|
N/A | N/A | N/A | |||
PCB-1242(53469-21-9)
|
N/A | N/A | N/A | |||
PCB-1248(12672-29-6)
|
N/A | N/A | N/A | |||
PCB-1254(11097-69-1)
|
N/A | N/A | N/A | |||
PCB-1260(11096-82-5)
|
N/A | 59% Rec (ML) | 46.64 % RSD (ML) | 50.00 ug/L | ||
Pentachlorobenzene(608-93-5)
|
10.000 ug/L | N/A | N/A | |||
Pentachloronitrobenzene(82-68-8)
|
20.000 ug/L | N/A | N/A | |||
Pentachlorophenol(87-86-5)
|
50.000 ug/L | 97% Rec (ML) | 38.66 % RSD (ML) | 50.00 ug/L | ||
Phenacetin(62-44-2)
|
20.000 ug/L | N/A | N/A | |||
Phenanthrene(85-01-8)
|
10.000 ug/L | 87% Rec (ML) | 15.50 % RSD (ML) | 50.00 ug/L | ||
Phenobarbitol(50-06-6)
|
10.000 ug/L | N/A | N/A | |||
Phenol(108-95-2)
|
10.000 ug/L | 46% Rec (ML) | 36.16 % RSD (ML) | 50.00 ug/L | ||
Phentermine(122-09-8)
|
N/A | N/A | N/A | |||
Phorate(298-02-2)
|
10.000 ug/L | N/A | N/A | |||
Phosalone(2310-17-0)
|
100.000 ug/L | N/A | N/A | |||
Phosmet(732-11-6)
|
40.000 ug/L | N/A | N/A | |||
Phosphamidon(13171-21-6)
|
100.000 ug/L | N/A | N/A | |||
Phthalic anhydride(85-44-9)
|
100.000 ug/L | N/A | N/A | |||
Piperonyl sulfoxide(120-62-7)
|
100.000 ug/L | N/A | N/A | |||
Pronamide(23950-58-5)
|
10.000 ug/L | N/A | N/A | |||
Propylthiouracil(51-52-5)
|
100.000 ug/L | N/A | N/A | |||
Pyrene(129-00-0)
|
10.000 ug/L | 84% Rec (ML) | 15.62 % RSD (ML) | 50.00 ug/L | ||
Pyridine(110-86-1)
|
N/A | N/A | N/A | |||
Pyridine, 3-chloromethyl-, hydrochloride(6959-48-4)
|
N/A | N/A | N/A | |||
Resorcinol(108-46-3)
|
100.000 ug/L | N/A | N/A | |||
Safrole(94-59-7)
|
10.000 ug/L | N/A | N/A | |||
Strychnine(57-24-9)
|
40.000 ug/L | N/A | N/A | |||
Sulfallate(95-06-7)
|
10.000 ug/L | N/A | N/A | |||
Sulfotepp(3689-24-5)
|
N/A | N/A | N/A | |||
Terbufos(13071-79-9)
|
20.000 ug/L | N/A | N/A | |||
Tetrachlorvinphos(22248-79-9)
|
20.000 ug/L | N/A | N/A | |||
Tetraethyl pyrophosphate(107-49-3)
|
40.000 ug/L | N/A | N/A | |||
Toluene-2,4-diisocyanate(584-84-9)
|
N/A | N/A | N/A | |||
Toxaphene(8001-35-2)
|
N/A | N/A | N/A | |||
Tri-p-tolyl phosphate(78-32-0)
|
10.000 ug/L | N/A | N/A | |||
Trifluralin(1582-09-8)
|
10.000 ug/L | N/A | N/A | |||
Trimethylphosphate(512-56-1)
|
10.000 ug/L | N/A | N/A | |||
Tris(2,3-dibromopropyl)phosphate(126-72-7)
|
200.000 ug/L | N/A | N/A | |||
Urethane(51-79-6)
|
N/A | N/A | N/A | |||
Volatile organic compounds(E-12419)
|
N/A | N/A | N/A | |||
Zinophos(297-97-2)
|
N/A | N/A | N/A | |||
alpha-BHC(319-84-6)
|
N/A | N/A | N/A | |||
alpha-Naphthylamine(134-32-7)
|
N/A | N/A | N/A | |||
alpha-Picoline(109-06-8)
|
N/A | N/A | N/A | |||
beta-BHC(319-85-7)
|
N/A | 85% Rec (ML) | 26.12 % RSD (ML) | 50.00 ug/L | ||
beta-Naphthylamine(91-59-8)
|
N/A | N/A | N/A | |||
bis(2-Chloroethoxy)methane(111-91-1)
|
10.000 ug/L | 102% Rec (ML) | 30.02 % RSD (ML) | 50.00 ug/L | ||
bis(2-Chloroethyl) ether(111-44-4)
|
10.000 ug/L | 83% Rec (ML) | 35.20 % RSD (ML) | 50.00 ug/L | ||
bis(2-Chloroisopropyl) ether(108-60-1)
|
10.000 ug/L | 98% Rec (ML) | 27.08 % RSD (ML) | 50.00 ug/L | ||
bis(2-Ethylhexyl) phthalate(117-81-7)
|
N/A | 82% Rec (ML) | 37.34 % RSD (ML) | 50.00 ug/L | ||
delta-BHC(319-86-8)
|
N/A | 27% Rec (ML) | 92.66 % RSD (ML) | 50.00 ug/L | ||
m-Cresol(108-39-4)
|
N/A | N/A | N/A | |||
o-Anisidine(90-04-0)
|
10.000 ug/L | N/A | N/A | |||
o-Cresol(95-48-7)
|
N/A | N/A | N/A | |||
o-Tolidine(119-93-7)
|
N/A | N/A | N/A | |||
o-Toluidine(95-53-4)
|
10.000 ug/L | N/A | N/A | |||
p,p'-DDT(50-29-3)
|
N/A | 72% Rec (ML) | 63.84 % RSD (ML) | 50.00 ug/L | ||
p-Benzoquinone(106-51-4)
|
10.000 ug/L | N/A | N/A | |||
p-Chloroaniline(106-47-8)
|
20.000 ug/L | N/A | N/A | |||
p-Cresidine(120-71-8)
|
10.000 ug/L | N/A | N/A | |||
p-Cresol(106-44-5)
|
N/A | N/A | N/A | |||
p-Dimethylaminoazobenzene(60-11-7)
|
N/A | N/A | N/A | |||
p-Nitroaniline(100-01-6)
|
20.000 ug/L | N/A | N/A | |||
p-Phenylenediamine(106-50-3)
|
N/A | N/A | N/A | |||
sym-Trinitrobenzene(99-35-4)
|
N/A | N/A | N/A |
Precision Descriptor Notes: | The precision and accuracy values were determined using regression equations derived from a 15 laboratory validation study. The study determined analytes using reagent water, drinking water, surface water, and industrial wastewaters with additions at six concentrations over the range 5 to 1300 ug/L. Single operator precision, overall precision, and accuracy were found to be directly related to the concentration of the parameter and essentially independent of the sample matrix. |
---|---|
Detection Level Note: | EQLs are estimated quantitation limits. |
Revision | PDF/Link |
---|---|
Revision 4.0, January 1998 |
The Water Quality Portal contains
sample results from
sites that use this method.
Download WQP data
Select data:
File format:
Sites where this method was used
Loading Sites ...